A simple and efficient established method that is characterized by its quickness and high sensitivity for determining ferrous ion in pure and pharmaceutical formulations by the generate of dark-blue precipitate using reaction of hexacyanoferrate(III) with ferrous ion in ammonium acetate medium. The equipment NAG-4SX3-3D analyzer was used to quantify turbidity by measuring the incident light attenuation crashing on the precipitate surface granules (0-180 degree). The optimum parameter has been investigated in order to improve the newly created approach's sensitivity.
The linear range (0.1-7) millimol.L-1 with (r=0.9971), (correlation coefficient), percentage linearity (R % = 99.42), and RSD % for the repetition (n=7) also were lower than 0.1 percent for the measurement of ferrous ion, with concentration (1, 4.7 millimol .L-1). Whereas L.O.D. = 212.6712 ng/sample from the progressive dilution throughout the calibration graph's lowest concentration linear dynamic range the suggested approach was compared to the traditional method (UV- spectrophotometric at λmax = 222 nm of analysis employing the conventional technique of adding by the use of paired t- test (the mean difference between pairs of measurements). It’s notice that with calculated numbers, there wasn't any substantial variation between the values given of any particular firm. t-value at 95% interval from the proposed approach.
Hameed, S., & Turkey, N. (2022). Determination of Ferrous Ion in Pure & Pharmaceutical Preparation by Continuous Flow Injection Analysis Via Turbidmetric Utilizing NAG-4SX3-3D Analyzer. Egyptian Journal of Chemistry, 65(131), 871-886. doi: 10.21608/ejchem.2022.131307.5788
MLA
Sarah Hameed; Nagham S Turkey. "Determination of Ferrous Ion in Pure & Pharmaceutical Preparation by Continuous Flow Injection Analysis Via Turbidmetric Utilizing NAG-4SX3-3D Analyzer". Egyptian Journal of Chemistry, 65, 131, 2022, 871-886. doi: 10.21608/ejchem.2022.131307.5788
HARVARD
Hameed, S., Turkey, N. (2022). 'Determination of Ferrous Ion in Pure & Pharmaceutical Preparation by Continuous Flow Injection Analysis Via Turbidmetric Utilizing NAG-4SX3-3D Analyzer', Egyptian Journal of Chemistry, 65(131), pp. 871-886. doi: 10.21608/ejchem.2022.131307.5788
VANCOUVER
Hameed, S., Turkey, N. Determination of Ferrous Ion in Pure & Pharmaceutical Preparation by Continuous Flow Injection Analysis Via Turbidmetric Utilizing NAG-4SX3-3D Analyzer. Egyptian Journal of Chemistry, 2022; 65(131): 871-886. doi: 10.21608/ejchem.2022.131307.5788
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