Abstract In this paper, some new bis-aryl hydrazone derivatives (4a-f) were prepared through the reaction of carboxylic acid hydrazides with 1,4-diacetylbenzene using classical methods, microwave and ultrasound irradiation methods. These compounds are obtained through a series of reactions where some carboxylic acids react with ethanol first in the presence of concentrated sulfuric acid to give the corresponding esters (2a-f), which when treatment with aqueous hydrazine give carboxylic acid hydrazides (3a-f).thus, The results proved that the use of microwave and ultrasound techniques is much better than the classical methods, as it gave a higher yield, shorter reaction time, and the absence of the use of solvents. All newly synthesized compounds were confirmed by IR, (1H & 13C) NMR spectral analysis and the corresponding reactions were monitored by TLC using the reported eluent
Mohammed, S. J., Sheat, A. M., Abood, S. A., & Yahya, O. M. (2021). Using Microwave and ultrasound to prepare of substituted Bis-acyl hydrazone Derivatives. Egyptian Journal of Chemistry, 64(11), 6423-6427. doi: 10.21608/ejchem.2021.78532.3842
MLA
Salim J. Mohammed; Attallah M. Sheat; Salih A. Abood; Omar M. Yahya. "Using Microwave and ultrasound to prepare of substituted Bis-acyl hydrazone Derivatives". Egyptian Journal of Chemistry, 64, 11, 2021, 6423-6427. doi: 10.21608/ejchem.2021.78532.3842
HARVARD
Mohammed, S. J., Sheat, A. M., Abood, S. A., Yahya, O. M. (2021). 'Using Microwave and ultrasound to prepare of substituted Bis-acyl hydrazone Derivatives', Egyptian Journal of Chemistry, 64(11), pp. 6423-6427. doi: 10.21608/ejchem.2021.78532.3842
VANCOUVER
Mohammed, S. J., Sheat, A. M., Abood, S. A., Yahya, O. M. Using Microwave and ultrasound to prepare of substituted Bis-acyl hydrazone Derivatives. Egyptian Journal of Chemistry, 2021; 64(11): 6423-6427. doi: 10.21608/ejchem.2021.78532.3842
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