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Egyptian Journal of Chemistry
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Volume Volume 62 (2019)
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Ghayad, I., El-Ansary, A., Abdel Aziz, Z., El-Akshr, A. (2019). Recovery of Zinc From Zinc Dross Using Pyrometallurgical and Electrochemical Methods. Egyptian Journal of Chemistry, 62(2), 103-133. doi: 10.21608/ejchem.2018.2782.1225
Ibrahim Mohamed Ghayad; Aida L. El-Ansary; Zeinab A. Abdel Aziz; Amany A. El-Akshr. "Recovery of Zinc From Zinc Dross Using Pyrometallurgical and Electrochemical Methods". Egyptian Journal of Chemistry, 62, 2, 2019, 103-133. doi: 10.21608/ejchem.2018.2782.1225
Ghayad, I., El-Ansary, A., Abdel Aziz, Z., El-Akshr, A. (2019). 'Recovery of Zinc From Zinc Dross Using Pyrometallurgical and Electrochemical Methods', Egyptian Journal of Chemistry, 62(2), pp. 103-133. doi: 10.21608/ejchem.2018.2782.1225
Ghayad, I., El-Ansary, A., Abdel Aziz, Z., El-Akshr, A. Recovery of Zinc From Zinc Dross Using Pyrometallurgical and Electrochemical Methods. Egyptian Journal of Chemistry, 2019; 62(2): 103-133. doi: 10.21608/ejchem.2018.2782.1225

Recovery of Zinc From Zinc Dross Using Pyrometallurgical and Electrochemical Methods

Article 15, Volume 62, Issue 2, February 2019, Page 103-133  XML
Document Type: Original Article
DOI: 10.21608/ejchem.2018.2782.1225
Authors
Ibrahim Mohamed Ghayad email 1; Aida L. El-Ansary2; Zeinab A. Abdel Aziz3; Amany A. El-Akshr4
1Corrosion Control & Surface Protection Lab., Metals Technology Dept., Central Metallurgical Research and Development Institute
2Dept. of chemistry, Faculty of Science, Cairo University
3CMRDI
4Higher Institute of Engineering at 15th May City, Egypt
Receive Date: 01 February 2018,  Revise Date: 21 March 2018,  Accept Date: 29 September 2018 
Abstract
Recovery of zinc from its dross was investigated using electrochemical and pyrometallurgical methods. Almost 100% pure zinc was obtained using these methods. A small bench scale system for the investigating the recovery of zinc using pyrometallurgical methods was developed. The system based on the evaporation of zinc (in the dross) at 1050oC and condensing zinc vapors into pure zinc in a separate crucible. Almost pure Zn (99.95%) is obtained using this method. Recovery of zinc was also performed using electrowinning from acidified zinc sulfate bath and electrorefining of zinc dross anodes in alkaline ammonia bath. In either method different parameters including current density and deposition time were addressed. Zinc powder of almost 100% purity was obtained.
Keywords
Zinc dross; hot dip galvanizing; electrorefining; electrowinning; pyrometallurical techniques
Main Subjects
Electrochemistry
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